Step by step instructions for Proton and Carbon. For a varian Unity/Inova 300. From University of Virginia
http://ernst.chem.virginia.edu/lutz/lutzinstruct.html
A fairly nice section on shimming. An section on basic data acquire, most varian new users need that.
http://biomol.uchsc.edu/researchFacilities/nmr/documentation/guide/contents.html
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